@article{oai:shizuoka.repo.nii.ac.jp:00000376, author = {長井, 洋一 and 和田, 秀樹}, journal = {静岡大学地球科学研究報告}, month = {Jul}, note = {application/pdf, A small-scale analytical technique for carbon and oxygen isotopic analyses of dolomite, siderite and magnesite was developed using a batch method. Carbonate samples were reacted with conc-phosphoric acid at 100℃ in vacuo. Using this batch method, standard calcite and dolomite samples were examined to check the minimum size of samples required. CO_2,gas greater than 10μl can be precisely measured with the conventional certainty. For smaller samples, isotopic results are affected by some contaminations evolved during reaction at 100℃ with phosphoric acid. Metamorphic calcite and dolomite collected from the Kasuga contact aureole, Gifu Pref. were examined using the small-scale analyses. Within a hand specimen size, a large oxygen isotopic heterogeneity up to 6‰ Was observed.}, pages = {25--34}, title = {微量ドロマイト試料同位体測定法の開発と応用}, volume = {19}, year = {1993} }